FACILITIES

Equipment

Below is a list of scientific equipment at the IAST. In addition to laboratory equipment, the IAST has a number of demonstration pilot resources: glass blowing pilot plant; biodiesel pilot plant; tyre recycling; rubberized asphalt cement and hot mix asphalt pilot plant; wood-plastic composites pilot plant; briquetting pilot plant; steam extraction pilot plant; solar drying pilot unit; biogas pilot plant; food/feed pilot extruder, etc.

Please click on the lab or department names below to view the associated equipment.

Differential Scanning Calorimeter
  • Measures the amount of energy absorbed or released by a sample when it is heated or cooled
  • Generate information about:
    • Amorphous and crystalline behavior
    • Polymorph and eutectic transitions
    • Curing and degree of cure
    • Many other material properties used to design, manufacture, and test products.
  • Has many industrial applications from pharmaceuticals and polymers, to nanomaterials and food products
  • Measures the amount of weight change of a material, either as a function of increasing temperature, or isothermally as a function of time
  • Samples can be analyzed in the form of powder or small pieces so the interior sample temperature remains close to the measured gas temperature
  • Inorganic material, metals, polymers and plastics, ceramics, glasses, and composite materials can be analyzed
  • Can be used to determine evaporation rates, which is used to measure the volatile emissions of liquid mixtures
  • Helps to identify plastics and organic materials by measuring the temperature of bond scissions in inert atmospheres or of oxidation in air or oxygen
Thermal Gravimetric Analyzer
Dynamic Mechanical Analyzer
  • Measures the mechanical properties of materials as a function of time, temperature, and frequency
  • Operates over a wide temperature range (-150 to 600°C)
  • Provides multiple modes of deformation including dual/single cantilever and 3-point bending, tension, compression, and shear
  • The clamps are individually calibrated for data accuracy
  • Measures flow and deformation of materials under applied forces and varying viscosity and viscoelasticity depending upon the external conditions applied, such as stress, strain, timescale and temperature
  • Applicable to all materials:
    • From fluids such as dilute solutions of polymers and surfactants through to concentrated protein formulations, to semi-solids such as pastes and creams, to molten or solid polymers.
Rheometer
Texture Analyzer
  • Measures texture and quantifies:
    • Hardness
    • Brittleness
    • Fracturability
    • Adhesiveness
    • Stiffness
    • Elasticity
    • Bloom Strength
  • Applicable for consumer products in:
    • Foods
    • Cosmetics
    • Pharmaceuticals
    • Chemicals
  • Measures the heat/energy created by a sample burned under an oxygen atmosphere in a closed vessel, which is surrounded by water, under controlled conditions
  • Generates information about:
    • Combustion
    • Calorific value
    • BTU value
Bomb Calorimeter

Analytic Instrumentation Laboratory

Hanna pH Meter
  • Measures the pH of a substance by its degree of acidity or alkalinity
  • Essentially calculates the electro-chemical potential between a known liquid inside the glass electrode (membrane) and an unknown liquid outside
  • It is a convenient measure of acidity / alkalinity of an aqueous solution at a specific temperature
  • Important for monitoring and controlling reactions, many of which only take place in a particular and sometimes narrow pH range
  • UV-Vis or UV/Vis refers to absorption spectroscopy or reflectance spectroscopy in the ultraviolet-visible spectral region
  • Used in analytical chemistry for the quantitative determination of different analytes, such as transition metal ions, highly conjugated organic compounds, and biological macromolecules
  • One of the best methods for determination of impurities in organic molecules
  • Useful in the structure elucidation of organic molecules, the presence or absence of unsaturation, the presence of hetero atoms
UV- VIS Ultraviolet Visible Spectrophotometry
Conductivity Meter
  • Measures the ability of a substance to conduct electric current
  • Conductivity measurements offer a rapid and non-destructive way to measure ion content in the sample
  • The measurement is made with an electronic sensor or meter in micro/milli-Siemens per centimeter or ppm
  • Conductivity is temperature sensitive and is typically standardized to 25°C
  • It is commonly used in hydroponics, aquaculture and freshwater systems to monitor the amount of nutrients, salts or impurities in the water
  • GC- Separation occurs as a result of unique equilibria established between the solutes and the stationary phase hence it separates the components of a mixture
  • This analytical method identifies different substances within a test sample by separating MS- Gas-phase ions  according to mass/charge ratio and are sequentially detected hence it characterizes each of the components individually
Gas Chromatography Mass Spectrometry
SpectrAA-5
  • Atomic absorption spectroscopy (AAS) is a procedure for the quantitative determination of chemical elements using the absorption of optical radiation (light) by free atoms in the gaseous state
  • It measure how well a sample absorbs light at each wavelength
  • Provides quantitative determination of different analytes, such as transition metal ions, highly conjugated organic compounds and biological macromolecules
  • Serves to control exposure to toxic, offensive or flammable vapours, gases and aerosols
  • Exhausts hazardous gases, dusts, mists, and vapours from a confined location and helps protect workers from inhalation exposure
Fume Hood
Cyanide Analyzer
  • Performs flow injection analysis of available cyanide and total cyanide in drinking water samples as well as in wastewater samples
  • Applicable in mining and industrial operations
  • Measures masses to four decimal places to the right of the decimal point (up to .0001 g)
  • Gives high degree of precision and accuracy in quantitative Chemistry
  • Extremely sensitive
Analytical Balance
Low Temperature Incubator
  • Precision Temperature Controlled Storage Device
  • Commonly used for applications such as B.O.D. determinations, plant and insect studies, fermentation studies, and bacterial culturing

Wet Organic Chemistry Lab

  • Used mainly for continuous distillation under reducing pressures
  • Removes volatile solvent from non-volatile or less volatile samples in a:
    • Fast
    • Efficient
    • Environmentally friendly manner
  • Used where the distillate is of high boiling point
  • It has high vacuum capability and can reduce operating temperature; has excellent mass and heat transfer and handles viscous fluids
  • The Single Stage Distillation Plant runs at 0.1 to 2.0 liters per hour, with shorter run times possible
  • It is invaluable in developing formulations, generating products and proving process separations involving Molecular Distillation Technology
  • This process could be used in many areas, including oleochemicals, fatty acids, biodiesel, fine chemicals, polymers, and pharmaceuticals

Wet Organic Chemistry Pilot Scale Facility

  • Has the ability to heat and stir at specific set points
  • Use to scale up reflux reactions for the Coconut oil Production
  • Can do reactions under pressure – like hydrogenations, carbonylations, formylations etc by adding hydrogen gas, carbon monoxide or a mixture or H2 & CO gases
  • Can be use to hydrogenate coconut oil to make coconut margarine

Bio-Diesel Facility

  • This boils water out of the oil
  • Has the ability to boil 1.5 drums of diesel at once
  • Provides the heat needed for the biodiesel creation process
  • Uses briquettes and small amounts of wood, mixed with either sawdust or Glycerol (A waste product of the biodiesel processing)
  • Consists of a boiler that transfers the energy using an oil circulator
  • Used to mix oil with methoxide
  • It is a two stage process
  • The reactor has a capacity of 120L of vegetable oil
  • Separates Biodiesel from Glycerol
  • Each has a capacity to hold 900L
  • Contains the Biodiesel from the Separation Tank
  • Contains aerators which uses air to wash (remove) sodium hydroxide from the biodiesel
  • This takes 48hrs and is repeated until desired quality is reached
  • Removes any remaining water
  • Process usually takes 1hr
  • The oil needs to reach 100C in order for the process to work
  • Stores biodiesel after the wash process and after the clarifier
  • Each has a capacity of 1700L
  • One of this is attached to each storage tank
  • Filters are used to ensure the quality of the biodiesel at every step of the process
  • Used at the fuel dispenser
  • The is to further ensure the biodiesel is of the desired quality and purity

Composite Materials Pilot Scale Facility

Reduces biomass into powder

This breaks down bottles and other waste plastic into small pieces

Dries the material

Mixes the plastic and the biomass

Melts and converts mixture into continuous noodle-like extrudates.

Compresses or molds the extruded material into pellets

  • Melts the pellets and molds it into a shape
  • Currently used for molding roofing tiles

Essential Oils Steam Extraction Pilot Facility

  • Extract Oils from:
    • Lemon grass
    • Orange Peel
  • Takes 1 1/2 hour to run each batch

Biogas Testing and Pilot Facility

  • Uses a slurry mix of 25% cow manure, 25% antelope grass and 50% water
  • Digester has a slurry capacity of 4800 Litres
  • Has the capacity to produce 2340 litres of gas (CH4) per day

Fabrication Shop

Used for:

  • Drilling Holes into workpieces
  • Reaming – Enlarging holes
  • Tapping – Putting threads into a hole

Used to bend sheets of metal

Used to join pieces of metal

Glass Blowing Facility

Used to display the different steps a sample of glass must go through before its final shape

Repairs and fabrication of small pieces of glass apparatuses are done on the bench

This is for bigger repairs and/or fabrication jobs that are too large for the bench

  • Used to grind glass
  • Applicable in smoothing the edges of the glass

This has a diamond-tipped blade for fast and accurate cutting of glass

Another tool used for applying the finishing touches to a piece of glass

Used for marking lines (gradations) or scribes on the glass

  • Glasses are brought to this machine after the Graduating Machine
  • This is then used to scribe on numbers and/or letters on to the piece of glass

Solar Dryer

Device that uses solar energy to dry substances, especially food

Recycled Rubber Facility and Rubberized Asphalt Cement Pilot Facility

  • The Tire De-beader has been specifically designed to remove steel beads from tires
  • The de-beader is a two part unit power by an electrical motor that rotates the tires and an air compressor that provide air to active the knife engagement cylinder and the spool life cylinder
  • A minimum of 120 psi air pressure is critical for effective operation of the de-beader. The capacity of the de-beader depends on the size of tire de-bead
  • The primary shredder consists a hopper and two counter rotating shafts power by two high power electrical motor that rotate on parallel axes, each shaft contains a series of cylindrical cutters
  • Cutting teeth are proportionally spaced around the circumference of each cylindrical cutter; the cylindrical cutters are spaced at proportional distances on the rotating shafts such that a cylindrical cutter on the first shaft rotates within a space between two identical cylindrical cutters on the second shaft
  • The size of the tire shreds produced in the primary shredding process can vary from 460mm to 100mm long and 230mm to 100mm wide
  • The granulator is a rugged, low profile, rotary cutting machine design to cut, chip and granulate the toughest materials with minimum horse power
  • It consists of a hopper bolted on top of the cutting chamber, the cutting chamber is a rectangular enclosure that carries the bed knives
  • The screen is supported below the rotor and act as a barrier to retain the material in the chamber until it achieves the particle size that will allow it to pass through the screen
  • The rotor is driven by a 100Hp electrical motor through belts

Transports materials automatically between stages

  • This blower utilizes impellers, which are typically flat plates with 4 – 10 blades arranged in a spoke pattern on one side, the flat plate mounts the impeller onto a shaft through a hub, or the point on the impeller from which the blades extend
  • The unit has a drive shaft, which is driven by a v-belt high speed electrical motor blowers
  •  The unit is housed by a circular welded assembly that is constructed from heavy-gauge sheet metal
  • When the impeller rotates, air is sucked into the input at the center of the centrifugal blower and forced out at a perpendicular outlet into the plenum, which is the airway through which air is forced out of the centrifugal fan’s output
  • The cyclone separator comprises a frame part, a cylindrical mantle part, an inlet outlet flow duct
  • The frame part of the cyclone separator is conical at its bottom portion; at the bottom of the conical portion, there is an outlet opening, which is provided with a paddle device power by an electrical motor, through which the rubber material is removed
  • Air and rubber first flows in a spiral pattern, beginning at the top of the cyclone and ending at the bottom end, the air and fibers exiting the cyclone in a straight stream through the center of the cyclone and out the top; the rubber particles in the rotating stream have too much inertia to follow the tight curve of the stream and strike the outside wall, falling then to the bottom of the cyclone where they can be removed
  • This removes the ferrous metal (wire) from the rubber particles in free-flowing processing systems
  • The unit is self cleaning and consists of drum and housing normally of stainless steel
  • The drum of the separator is designed in such a way that only half of its side is magnetized and the other half is not
  • The rubber particles materials from the cyclone enter the top of the magnetic drum separator and flows across the surface of the drum, the rotating drum in the magnetic field captures the wire whereas rubber particles fall free from the drum into a chute, as the drum rotates, the wire captured is carried past the diverter and released outside of the magnetic field
  • This separator is made on a porous deck surface of fabric woven wire
  • Upon this surface, the rubber material to be separated is stratified by air discharge through the deck from an air supply system built into the machine base
  • The heavy rubber particles sink to the bottom of the fluidized material bed on the deck, the straight line vibrating motion, imparted on the deck by the eccentric drive carries the heavy particles away from the light particle which floats in the air stream
  • The deck is sloped in two direction so that the lightest particles float down towards the lower discharge corner, the heaviest particles are conveyed up the slope and forced off the deck at its upper point
  • This separator is a screening device designed to separate smaller particles from larger particles and to remove fibers
  • The separator consists of a screen, approximately 48 or 60 inches in diameter fited into a steel frame, the frames are attached to a spring supported table which contains the motor and eccentric weight system
  • The machine is driven by a motor designed to transmit vibration to the screen, this vibration causes smaller particles to drop through the screen while larger oversize particles pass off the top of the screen
  • Mixes asphalt and recycled rubber to form rubberized asphalt
  • Attached to the top of the kiln

Produces heat for the reaction process

Biomass Briquette Pilot Facility

  • Reduces moisture content of biomass
  • Processes 300 – 400kg/h

Compresses biomass to form briquettes

Compressed Clay Block Pilot Facility

Compresses the mixture from the extruder into blocks

Fired Clay Aggregate Pilot Facility

  • Mixes clay, stabilizers, water and sand
  • Also used to create clay aggregates for the fired clay aggregate project

Used to remove moisture from the clay

Food Extruder

State of the art multifunction co-rotating twin screw Extruder with:

  • Clamp barrel
  • Variable processing time
  • Interchangeable screw element
  • Electrical heating / water cooling
  • Processing temperature up to 400 0C
  • Vertical screw feeder
INSTITUTE OF APPLIED SCIENCE AND TECHNOLOGY
UNIVERSITY OF GUYANA CAMPUS,
TURKEYEN, GREATER GEORGETOWN,
GUYANA
TELEPHONE: (592) 222-4212-5, (592)-222-4218, (592)-222-5864
FAX: (592) 222-4229

For further information kindly contact:

Mr. DEONARINE JAGDEO
Director (ag.)


RAYANN HINCKSON
Confidential Secretary
r.hinckson@iast.gov.gy